Template based precursor route for the synthesis of CuInSe2 nanorod arrays for potential solar cell applications.
Identifieur interne : 000334 ( Main/Exploration ); précédent : 000333; suivant : 000335Template based precursor route for the synthesis of CuInSe2 nanorod arrays for potential solar cell applications.
Auteurs : RBID : pubmed:24367756Abstract
Polycrystalline CuInSe2 (CISe) nanorods are promising for the fabrication of highly efficient active layers in solar cells. In this work we report on a nanocasting approach, which uses track-etched polycarbonate films as hard templates for obtaining three-dimensionally (3D) arranged CISe nanorod arrays. Copper and indium ketoacidoximato complexes and selenourea were employed as molecular precursors. Arrays of parallel isolated cylindrical pores of 100 nm nominal diameter and 5 μm length were used for the infiltration of the precursor solution under inert atmosphere, followed by drying, thermal conversion into a preceramic 'green body', a subsequent dissolution of the template, and a final thermal treatment at 450 °C. The nanorods that where synthesised in this way have dimensions equal to the pore sizes of the template. Investigation of the CuInSe2 nanorod samples by spectroscopic and diffraction methods confirmed a high purity and crystallinity, and a stoichiometric composition of the CISe ternary semiconductor compound.
DOI: 10.3762/bjnano.4.98
PubMed: 24367756
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Bang</name><affiliation wicri:level="3"><nlm:affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</nlm:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt</wicri:regionArea><placeName><region type="land" nuts="1">Hesse (Land)</region><region type="district" nuts="2">District de Darmstadt</region><settlement type="city">Darmstadt</settlement></placeName></affiliation></author><author><name sortKey="Gora, Niklas S A" uniqKey="Gora N">Niklas S A Gora</name><affiliation wicri:level="3"><nlm:affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</nlm:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt</wicri:regionArea><placeName><region type="land" nuts="1">Hesse (Land)</region><region type="district" nuts="2">District de Darmstadt</region><settlement type="city">Darmstadt</settlement></placeName></affiliation></author><author><name sortKey="Balog, Ildiko" uniqKey="Balog I">Ildiko Balog</name><affiliation wicri:level="3"><nlm:affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</nlm:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt</wicri:regionArea><placeName><region type="land" nuts="1">Hesse (Land)</region><region type="district" nuts="2">District de Darmstadt</region><settlement type="city">Darmstadt</settlement></placeName></affiliation></author><author><name sortKey="Hoffmann, Rudolf C" uniqKey="Hoffmann R">Rudolf C Hoffmann</name><affiliation wicri:level="3"><nlm:affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</nlm:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt</wicri:regionArea><placeName><region type="land" nuts="1">Hesse (Land)</region><region type="district" nuts="2">District de Darmstadt</region><settlement type="city">Darmstadt</settlement></placeName></affiliation></author><author><name sortKey="Schneider, J Rg J" uniqKey="Schneider J">Jörg J Schneider</name><affiliation wicri:level="3"><nlm:affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</nlm:affiliation><country xml:lang="fr">Allemagne</country><wicri:regionArea>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt</wicri:regionArea><placeName><region type="land" nuts="1">Hesse (Land)</region><region type="district" nuts="2">District de Darmstadt</region><settlement type="city">Darmstadt</settlement></placeName></affiliation></author></titleStmt><publicationStmt><date when="2013">2013</date><idno type="doi">10.3762/bjnano.4.98</idno><idno type="RBID">pubmed:24367756</idno><idno type="pmid">24367756</idno><idno type="wicri:Area/Main/Corpus">000237</idno><idno type="wicri:Area/Main/Curation">000237</idno><idno type="wicri:Area/Main/Exploration">000334</idno></publicationStmt></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Polycrystalline CuInSe2 (CISe) nanorods are promising for the fabrication of highly efficient active layers in solar cells. In this work we report on a nanocasting approach, which uses track-etched polycarbonate films as hard templates for obtaining three-dimensionally (3D) arranged CISe nanorod arrays. Copper and indium ketoacidoximato complexes and selenourea were employed as molecular precursors. Arrays of parallel isolated cylindrical pores of 100 nm nominal diameter and 5 μm length were used for the infiltration of the precursor solution under inert atmosphere, followed by drying, thermal conversion into a preceramic 'green body', a subsequent dissolution of the template, and a final thermal treatment at 450 °C. The nanorods that where synthesised in this way have dimensions equal to the pore sizes of the template. Investigation of the CuInSe2 nanorod samples by spectroscopic and diffraction methods confirmed a high purity and crystallinity, and a stoichiometric composition of the CISe ternary semiconductor compound.</div></front></TEI><pubmed><MedlineCitation Owner="NLM" Status="PubMed-not-MEDLINE"><PMID Version="1">24367756</PMID><DateCreated><Year>2013</Year><Month>12</Month><Day>24</Day></DateCreated><DateCompleted><Year>2013</Year><Month>12</Month><Day>24</Day></DateCompleted><DateRevised><Year>2014</Year><Month>01</Month><Day>24</Day></DateRevised><Article PubModel="Electronic-eCollection"><Journal><ISSN IssnType="Electronic">2190-4286</ISSN><JournalIssue CitedMedium="Print"><Volume>4</Volume><PubDate><Year>2013</Year></PubDate></JournalIssue><Title>Beilstein journal of nanotechnology</Title><ISOAbbreviation>Beilstein J Nanotechnol</ISOAbbreviation></Journal><ArticleTitle>Template based precursor route for the synthesis of CuInSe2 nanorod arrays for potential solar cell applications.</ArticleTitle><Pagination><MedlinePgn>868-74</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.3762/bjnano.4.98</ELocationID><Abstract><AbstractText>Polycrystalline CuInSe2 (CISe) nanorods are promising for the fabrication of highly efficient active layers in solar cells. In this work we report on a nanocasting approach, which uses track-etched polycarbonate films as hard templates for obtaining three-dimensionally (3D) arranged CISe nanorod arrays. Copper and indium ketoacidoximato complexes and selenourea were employed as molecular precursors. Arrays of parallel isolated cylindrical pores of 100 nm nominal diameter and 5 μm length were used for the infiltration of the precursor solution under inert atmosphere, followed by drying, thermal conversion into a preceramic 'green body', a subsequent dissolution of the template, and a final thermal treatment at 450 °C. The nanorods that where synthesised in this way have dimensions equal to the pore sizes of the template. Investigation of the CuInSe2 nanorod samples by spectroscopic and diffraction methods confirmed a high purity and crystallinity, and a stoichiometric composition of the CISe ternary semiconductor compound.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Pashchanka</LastName><ForeName>Mikhail</ForeName><Initials>M</Initials><Affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</Affiliation></Author><Author ValidYN="Y"><LastName>Bang</LastName><ForeName>Jonas</ForeName><Initials>J</Initials><Affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</Affiliation></Author><Author ValidYN="Y"><LastName>Gora</LastName><ForeName>Niklas S A</ForeName><Initials>NS</Initials><Affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</Affiliation></Author><Author ValidYN="Y"><LastName>Balog</LastName><ForeName>Ildiko</ForeName><Initials>I</Initials><Affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</Affiliation></Author><Author ValidYN="Y"><LastName>Hoffmann</LastName><ForeName>Rudolf C</ForeName><Initials>RC</Initials><Affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</Affiliation></Author><Author ValidYN="Y"><LastName>Schneider</LastName><ForeName>Jörg J</ForeName><Initials>JJ</Initials><Affiliation>Fachbereich Chemie, Eduard-Zintl-Institut, Fachgebiet Anorganische Chemie, Technische Universität Darmstadt, Petersenstraße 18, 64287 Darmstadt, Germany.</Affiliation></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType>Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2013</Year><Month>12</Month><Day>10</Day></ArticleDate></Article><MedlineJournalInfo><Country>Germany</Country><MedlineTA>Beilstein J Nanotechnol</MedlineTA><NlmUniqueID>101551563</NlmUniqueID><ISSNLinking>2190-4286</ISSNLinking></MedlineJournalInfo><OtherID Source="NLM">PMC3869223</OtherID><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">CIS</Keyword><Keyword MajorTopicYN="N">light absorption</Keyword><Keyword MajorTopicYN="N">nanocasting</Keyword><Keyword MajorTopicYN="N">nanorod arrays</Keyword><Keyword MajorTopicYN="N">precursor synthesis</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="ecollection"><Year>2013</Year><Month></Month><Day></Day></PubMedPubDate><PubMedPubDate PubStatus="received"><Year>2013</Year><Month>8</Month><Day>28</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2013</Year><Month>12</Month><Day>1</Day></PubMedPubDate><PubMedPubDate PubStatus="epublish"><Year>2013</Year><Month>12</Month><Day>10</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2013</Year><Month>12</Month><Day>25</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2013</Year><Month>12</Month><Day>25</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2013</Year><Month>12</Month><Day>25</Day><Hour>6</Hour><Minute>1</Minute></PubMedPubDate></History><PublicationStatus>epublish</PublicationStatus><ArticleIdList><ArticleId IdType="doi">10.3762/bjnano.4.98</ArticleId><ArticleId IdType="pubmed">24367756</ArticleId><ArticleId IdType="pmc">PMC3869223</ArticleId></ArticleIdList></PubmedData></pubmed></record>Pour manipuler ce document sous Unix (Dilib)
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